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Title: Growth of large SbSI crystals
Authors: Szperlich, Piotr
Toroń, Bartłomiej
Nowak, Marian
Jesionek, Marcin
Kępińska, Mirosława
Bogdanowicz, Włodzimierz
Keywords: antimony sulfoiodide; crystal growth; vapour growth process; nanomaterials
Issue Date: 2014
Citation: Materials Science-Poland, 2014, iss. 4, s. 669-675
Abstract: In this paper a novel method of SbSI single crystals fabrication is presented. In this method a sonochemically prepared SbSI gel is used as an intermediate product in a vapour growth process. The main advantages of the presented technique are as follows. First, the SbSI gel source material has lower temperature of sublimation and allows to avoid explosions during SbSI synthesis (the sonochemical synthesis is free of any explosion hazard). Second, but not least, the grown SbSI single crystals have smaller ratio of longitudinal and lateral dimensions. The cross sections of the presented crystals are relatively large (they are up to 9 mm2). The crystals have been characterized by X-ray diffraction, angle-resolved optical spectroscopy, and diffusive reflectivity.
DOI: 10.2478/S13536-014-0247-4
ISSN: 2083-1331
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