http://hdl.handle.net/20.500.12128/9364
Tytuł: | Identification and characterization of new designer drug 4-fluoro-PV9 and [alfa]-PHP in the seized materials |
Autor: | Majchrzak, Milena Rojkiewicz, Marcin Celiński, Rafał Kuś, Piotr Sajewicz, Mieczysław |
Słowa kluczowe: | Designer drugs; 4-Fluoro-PV9; a-PHP; ESI-MS/MS; GC–MS; NMR |
Data wydania: | 2016 |
Źródło: | Forensic Toxicology, 2016, iss. 1, s. 115-124 |
Abstrakt: | In this study, we present identification and physicochemical characterization of new cathinone derivatives, 4-fluoro-PV9 and already known a-PHP in seized materials. Although the disclosure of a-PHP from an illegal product had been reported and characterized to some extent, the data on a-PHP are also presented together with those of 4-fluoro-PV9. The data of characterization for the two compounds were obtained by high-performance liquid chromatography (HPLC)–mass spectrometry and HPLC– diode array detection, electrospray ionization/ion trap mass spectrometry in MS2 and MS3 modes, gas chromatography– mass spectrometry, thermogravimetric analysis, differential scanning calorimetry, Fourier transform infrared spectroscopy, ultraviolet-visible spectroscopy, and nuclear magnetic resonance spectroscopy. To our knowledge, this is the first report for identification and detailed characterization of 4-fluoro-PV9 circulated on the illegal drug market. |
URI: | http://hdl.handle.net/20.500.12128/9364 |
DOI: | 10.1007/s11419-015-0295-4 |
ISSN: | 1860-8965 |
Pojawia się w kolekcji: | Artykuły (WNŚiT) |
Plik | Opis | Rozmiar | Format | |
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Majchrzak_Identification_and_characterization_of_new_designer_drug.pdf | 1,32 MB | Adobe PDF | Przejrzyj / Otwórz |
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