DOE Application for Analysis of Tribological Properties of the Al2O3/IF-WS2 Surface Layers

Abstract

The article presents the effect of the processing parameters on tribological properties of aluminum oxide coatings Al2O3 doped with fullerene-like tungsten disulfide (IF-WS2) by design of experiment (DOE). Anodic oxidation of aluminum alloy was carried out in a ternary solution of SAS (sulfuric, adipic and oxalic acids) with IF-WS2. The thickness, geometric structure of the surface (SGP) and the tribological properties such as friction coefficient of tribological pair: Al2O3/IF-WS2 with polieteroeteroketon filled with graphite, carbon fiber and PTFE (named PEEK/BG) were investigated. The influence of electrolysis time and temperature on the tribological properties of coatings was studied using 2k factorial design. The stabilization of the friction coefficient indicates generation of steady anti-wear and anti-seizure Al2O3/IF-WS2 oxide coatings. DOE suggest i.e. high positive correlation between oxide thickness and time and temperature of the anodizing process.